Spectrophotometric and AAS Determinations of Trace Zinc (II) in Natural Waters and Human Blood after Preconcentration with Phenanthraquinone Monophenylthiosemicarbazone.

Spectrophotometric and AAS determinations of trace zinc(II) in natural waters and human blood after preconcentration with phenanthraquinone monophenylthiosemicarbazone.

Selective flotation-spectrophotometric determination of trace copper(II) in natural waters, human blood and drug samples using phenanthraquinone monophenylthiosemicarbazone.

Copper(II) forms 1:1 and 1:2 intense red complexes with phenanthraquinone monophenylthiosemicarbazone (PPT) at pH 3-3.5 and > or =6.5, respectively. These complexes exhibit maximal absorbance at 545 and 517 nm, the molar absorptivity being 2.3 x 10(4) and 4.8 x 10(4) l mol(-1) cm(-1), respectively. However, the 1:1 complex was quantitatively floated with oleic acid (HOL) surfactant in the pH ra...

Preconcentration based dispersive liquid-liquid microextraction for spectrophotometric determination of zinc in natural water and human blood after multivariate optimization based on Box-Behnken design

A new simple and rapid dispersive liquid-liquid microextraction has been applied to preconcentrate tracelevels of zinc as a prior step to its determination by spectrophotometric method. In the proposed method, 4-(2-pyridylazo) resorcinol (PAR) is used as a chelating agent, and chloroform and ethanol are selected asextraction and dispersive solvent. The optimization strategy is carried out by us...

comparison of blood flow velocity changes in posterior cerebral artery measured with transcranial doppler sonography in migraineurs with visual aura and normal persons after photostimulation

چکیده ندارد.

preconcentration based dispersive liquid-liquid microextraction for spectrophotometric determination of zinc in natural water and human blood after multivariate optimization based on box-behnken design

a new simple and rapid dispersive liquid-liquid microextraction has been applied to preconcentrate tracelevels of zinc as a prior step to its determination by spectrophotometric method. in the proposed method, 4-(2-pyridylazo) resorcinol (par) is used as a chelating agent, and chloroform and ethanol are selected asextraction and dispersive solvent. the optimization strategy is carried out by us...